Transmission Electron Microscopic Study of Tetracalcium Phosphate Surface-Treated in Diammonium Hydrogen Phosphate Solution
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Transmission Electron Microscopic Study of Tetracalcium Phosphate Surface-Treated in Diammonium Hydrogen Phosphate Solution
The present study investigates the changes in microstructure and microchemistry (particularly Ca/P ratio) during whisker formation on the surface of a monolithic TTCP powder in a basic phosphoric acid solution. The XRD results indicate that when TTCP powder was treated for 10min or less in (NH4)2HPO4 solution, the monolithic TTCP phase remains unchanged. When treated for 30min, apatite whiskers...
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The present study investigates the changes in microstructure and microchemistry (particularly Ca/P ratio) during whisker formation on the surface of TTCP powder in hydrochloric solution. XRD results indicate that the as-fabricated (non-treated) powder has a monolithic TTCP crystal structure. When the powder is treated for 10min in HCl, a DCPD phase appears on TTCP surface, which increases in in...
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Six different tetracalcium phosphate (TTCP) products were synthesized by solid state reaction at high temperature by varying the overall calcium to phosphate ratio of the synthesis mixture. The objective was to evaluate the effect of the calcium to phosphate ratio on a TTCP-dicalcium phosphate dihydrate (DCPD) cement. The resulting six TTCP-DCPD cement mixtures were characterized using X-ray di...
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ژورنال
عنوان ژورنال: MATERIALS TRANSACTIONS
سال: 2005
ISSN: 1345-9678,1347-5320
DOI: 10.2320/matertrans.46.885